Microwave-assisted synthesis and characterization of novel metal-free and metallophthalocyanines containing four 14-membered tetraaza macrocycles
Citation
Bıyıklıoğlu, Z., Kantekin, H. & Özil, M. (2007). Microwave-assisted synthesis and characterization of novel metal-free and metallophthalocyanines containing four 14-membered tetraaza macrocycles. Journal of Organometallic Chemistry, 692(12), 2436-2440. https://doi.org/10.1016/j.jorganchem.2007.02.013Abstract
The novel tetrasubstituted metal-free phthalocyanine (6) and metallophthalocyanines (7, 8) bearing four 14-membered tetraaza macrocycles moieties on peripheral positions have been synthesized by cyclotetramerization reaction of phthalonitrile derivative (5) in a multi-step reaction sequence. The new compounds were characterized by a combination of IR, 1H NMR, 13C NMR, UV-vis, elemental analysis and MS spectral data. © 2007 Elsevier B.V. All rights reserved.
