Güncel Gönderiler: FEF, Kimya Bölümü Koleksiyonu
Toplam kayıt 481, listelenen: 201-220
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Characterization and pillaring of a Turkish bentonite (Resadiye)
(Elsevier, 2007)The shifts of the Si{single bond}O{single bond}Si stretching and the Si{single bond}O{single bond}Al and Si{single bond}O{single bond}Si bending modes, as well as the free silica peak in the IR spectra and the strengthening ... -
4-(4-Allyl-2-meth-oxyphen-oxy)benzene-1,2-dicarbonitrile
(Wiley, 2007)In the title compound, C18H14N2O2, the dihedral angle between the two benzene rings is 88.6 (1)°. The allyl group is disordered over two orientations, with refined occupancies of 0.695 (6) and 0.305 (6). The meth-oxy group ... -
Microwave-assisted and conventional synthesis of new phthalocyanines containing 4-(p-fluorophenyl)-3-methyl-4,5-dihydro-1H-1,2,4-triazol-5-one moieties
(Elsevier, 2007)New metal-free and metal (Zn, Ni, Cu and Co) phthalocyanines containing 4-(p-fluorophenyl)-3-methyl-4,5-dihydro-1H-1,2,4-triazol-5-one moiety have been prepared from 1-(3,4-dicyanophenyl)-4-(p-fluorophenyl)-3-methyl-4,5- ... -
Synthesis of some N-alkoxycarbonyl-N"-benzoyl-benzamidrazones(p- toluamidrazones) and 1,3,5-trisubstituted 1,2,4-triazole derivatives from N-benzoylimidates and their antimicrobial and anticancer screening studies
(Wiley, 2007)Some new N-alkoxycarbonyl-N?-benzoyl-benzamidrazones (p-toluamidrazones) 3a-3d, and 1,3,5-trisubstituted 1,2,4-triazole 4a-4h derivatives by starting from N-benzoylbenzimidates or N-benzoyl-p-toluimidates. The structures ... -
Microwave-assisted synthesis and characterization and theoretical calculations of the first example of free and metallophthalocyanines from salen type Schiff base derivative bearing thiophen and triazole heterocyclic rings
(Elsevier, 2007)Novel metal-free and metallophthalocyanine complexes of Co, Ni, Cu, and Zn have been synthesized by exposure to microwave irradiation and reflux conditions and the products purified by several techniques. The newly prepared ... -
5,5-Diethylbarbiturate complexes of silver with 2,2′-bipyridine and 3-(2-pyridyl)propanol: Syntheses, crystal structures, spectroscopic, thermal and antimicrobial activity studies
(Verlag der Zeitschrift fur Naturforschung, 2008)Two silver 5,5-diethylbarbiturate (barb) complexes with 2,2?-bipyridine (bpy) and 3-(2-pyridyl) propanol (pypr), [Ag(barb)(bpy)] (1) and [Ag(barb)(pypr)] (2), have been prepared and characterized by elemental analysis, IR ... -
The microwave-assisted synthesis and characterization of novel polymeric phthalocyanines containing resorcinarene
(Elsevier, 2008)Novel metal phthalocyanine (Cu, Zn, Co, Ni) polymers containing resorcinarene moieties were prepared; the resorcinarene was obtained by the acid-catalysed cyclocondensation of resorcinol and acetaldehyde under microwave ... -
Synthesis and crystal structure of N-(3-methyl-5-phenyl-3,5-dihydro-4H-1,2,4-triazol-4-yl)benzamide
(Japan Society for Analytical Chemistry, 2008)The title compound, N-(3-methyl-5-phenyl-3,5-dihydro-4H-1,2,4-triazol-4-yl)benzamide, C16H14N4O, crystallizes in the monoclinic space group P21/c with the following unit cell parameters: a = 10.6011(6)Å, b = 7.5676(4)Å, c ... -
Synthesis and anticancer evaluation of some new 4-amino-3-(p-methoxybenzyl) -4,5-dihydro-1,2,4-triazole-5-one derivatives
(Verlag der Zeitschrift fur Naturforschung, 2008)4-Amino-3-p-methoxybenzyl-5-oxo-4,5-dihydro-1,2,4-triazol-1-yl-acetic acid ethyl ester (2) was prepared from 4-amino-4,5-dihydro-1H-1,2,4-triazole-5-one (1) and ethyl bromoacetate. Compound 3 was synthesized by the ... -
Studies on the protonation constants of some triazoles in ethanol-water mixtures
(Chemical Publishing Co., 2008)Several studies, involving the formation and investigation of biological activities of some triazoles derivatives. These derivatives have weak acidic properties. To gain more information about the effect of solvent on ... -
Reversible immobilization of catalase by using a novel bentonite-cysteine (Bent-Cys) microcomposite affinity sorbents
(Elsevier, 2008)This study focused on developing bentonite-cysteine (Bent-Cys) microcomposite affinity sorbents (38-105 ?m) for catalase adsorption from aqueous solutions. Pseudo-biospecific affinity ligand l-cysteine was covalently binded ... -
Binuclear transition metal complexes of a novel lateral ‒N-methylthiosemicarbazone through the central ethylene bridge: Synthesis, structural characterization and the response of ligand molecule to different solvent media
(Elsevier, 2008)The condensation of 2,2?-(2,3-bis((1-formylnaphthalen-2-yloxy)methyl)but-2-ene-1,4-diy l)bis(oxy)di-1-naphthaldehyde with 4-methyl thiosemicarbazide gave a novel N-methylthiosemicarbazone and then the reaction of this ... -
Synthesis, potentiometric titrations and antioxidant activities of some 4-acylamino-4,5-dihydro-1H-1,2,4-triazol-5-one derivatives
(2008)Five novel 3-alkyl-4-cinnamoylamino-4,5-dihydro-1H-1,2,4-triazol-5-ones (2) were synthesized by the reactions of 3-alkyl-4-amino-4,5-dihydro-1H-1,2,4- triazol-5-ones (1) with cinnamoyl chloride and characterized by elemental ... -
Ni(II), Cu(II), and Zn(II) complexes of tetradentate schiff base containing two thiadiazoles units: Structural, spectroscopic, magnetic properties, and molecular modeling studies
(Wiley, 2008)Four new mononuclear metal complexes with a mononucleating Schiff base ligand containing two thiadiazoles units have been synthesized. The ligand and metal complexes were characterized by elemental analyses, IR, 1H, and ... -
Microwave-assisted synthesis and antifungal activity of some new 1H-1,2,4-triazole derivatives
(Springer, 2008)A number of 3-aryl-4-arylmethylideneamino-4,5-dihydro-1H-1,2,4-triazol-5- ones were synthesized by reaction of the corresponding aromatic aldehydes with 4-amino-3-aryl-1H-1,2,4-triazol-5-ones in anhydrous ethanol under ... -
Structural analysis of reactive dye species retained by the basic alumina surface
(Springer, 2009)The alumina-dye composites were prepared by treating the basic alumina with the water solutions of Reactive Red 120 (RR 120) and Reactive Blue 15 (RB 15) dyes. The bands of low intensities in the 1400-1600 cm-1 region and ... -
Determination of adsorptive properties of a Turkish Sepiolite for removal of Reactive Blue 15 anionic dye from aqueous solutions
(Elsevier, 2009)Reactive Blue 15 (RB 15) adsorption on the Turkish Sepiolite was carried out by batch equilibrium technique. IR spectrum and surface area measurement of the composite of dye-sepiolite (Turkish) pointed out that dye species ... -
Determination of the protonation constants of triazole derivatives in non-aqueous solvents
(2009)Different 17 triazole derivatives were titrated with tetrabutylammonium hydroxide in four non-aqueous solvents (isopropyl alcohol, rert-butyl alcohol, N,N-dimethylformamide and acetonitrile), using Potentiometric method. ... -
Synthesis of 1,2,4-Triazole derivatives and determination of protonation constant
(2009)A microwave irradiation method has been developed for the synhesis of some 1,2,4-triazole derivatives using environmentally benign solvent ethanol in open vessels. Twelve 1,2,4-triazole derivatives were synthesized in good ... -
Synthesis of methyl (E)-2′,4″-thiazachalcones and their N-alkyl derivatives, photochemistry with theoretical calculations and antimicrobial activities
(TUBİTAK, 2009)A series of 9 new (E) -thiazachalcones (1-3), and their N -alkyl substituted derivatives (4-6), and stereoselective dimerization products (7-9) were synthesized, then tested for antimicrobial activity against all test ...
